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Köp båda 2 för 1049 kr1. Introduction.- 1.1. Why Transient Techniques?.- 1.2. The Electrical Double Layer.- 1.3. The Kinetics of Charge Transfer Processes in the Steady State.- 1.3.1. Simple Charge Transfer Reactions.- 1.3.2. Complex Charge Transfer Reactions.- 1.4. General Current Equation.- 1.5. Surface Heterogeneity.- 1.6. Electrochemical Adsorption and Pseudocapacitance.- 2. Experimental Methods.- 2.1. Types of Perturbation.- 2.2. Cell and Electrode Design.- 2.2.1. Cell Design.- 2.2.2. Working-Electrode Design.- 2.2.3. Solution Preparation.- 2.3. The Electronics of Electrochemistry.- 2.3.1. Operational Amplifiers.- 2.3.2. The Voltage Follower.- 2.3.3. The Current Follower.- 2.3.4. The Voltage Adder.- 2.3.5. The Integrator.- 2.3.6. The Frequency Response of Operational Amplifiers.- 2.4. Potentiostats.- 2.4.1. Circuit Design.- 2.4.2. IR Compensation.- 2.5. Galvanostats.- 2.6. Transient Response.- 2.6.1. Introduction.- 2.6.2. Transform Analysis.- 3. The Mathematics of Diffusion.- 3.1. Introduction.- 3.2. Fick's Laws of Diffusion.- 3.3. Laplace Transforms.- 3.4. Laplace Transformation of Fick's Second Law.- 3.4.1. Planar Diffusion.- 3.4.2. Spherical Diffusion.- 3.4.3. Cylindrical Diffusion.- 3.4.4. Diffusion to an Expanding Plane.- 3.4.5. Initial and Boundary Conditions.- 3.5. Coupled Chemical/Electrochemical Processes.- 3.6. Inverse Laplace Transformation.- 3.7. Analysis in Laplace Space.- 3.8. Numerical Analysis.- 3.9. Digital Simulation.- 3.10. Analog Methods.- 4. Potential Step Chronoamperometry and Chronocoulometry.- 4.1. Introduction.- 4.2. Experimental.- 4.3. Simple Charge Transfer Reactions.- 4.3.1. Reversible Reactions.- 4.3.2. Irreversible Reactions.- 4.3.3. Quasi-Reversible Reactions.- 4.3.4. Metal Dissolution Reactions.- 4.3.5. Cyclic Potential Step Methods.- 4.4. Coupled Chemical/Electrochemical Processes.- 4.4.1. The CE Mechanism.- 4.4.2. The EC Mechanism.- 4.4.3. The ECE Mechanism.- 4.4.4. The Catalytic Mechanism.- 4.5. The Voltage Step Method.- 5. Chronopotentiometry.- 5.1. Introduction.- 5.2. Experimental.- 5.3. Simple Charge Transfer Reactions.- 5.3.1. Reversible Reactions.- 5.3.2. Irreversible Reactions.- 5.3.3. Quasi-Reversible Reactions.- 5.3.4. Parallel Charge Transfer Reactions.- 5.3.5. Consecutive Charge Transfer Reactions.- 5.3.6. Adsorption.- 5.4. Coupled Chemical/Electrochemical Processes.- 5.4.1. The CE Mechanism.- 5.4.2. The EC Mechanism.- 5.4.3. The ECE Mechanism.- 5.4.4. The Catalytic Mechanism.- 5.5. Current Reversal and Cyclic Methods.- 5.5.1. Current Reversal Techniques.- 5.5.2. Cyclic Techniques.- 5.6. Other Current Wave Forms.- 6. Linear Potential Sweep and Cylic Voltammetry.- 6.1. Introduction.- 6.2. Experimental.- 6.3. Double Layer Charging.- 6.4. Simple Charge Transfer Reactions.- 6.5. Coupled Chemical/Electrochemical Processes.- 6.5.1. The CE Mechanism.- 6.5.2. The EC Mechanism.- 6.5.3. The ECE Mechanism.- 6.5.4. The Catalytic Mechanism.- 6.5.5. Diagnostic Criteria.- 6.6. Adsorption.- 6.7. Convolution Potential Sweep Voltammetry.- 7. AC Impedance Techniques.- 7.1. Introduction.- 7.2. Experimental.- 7.2.1. AC Bridge Methods.- 7.2.2. Phase-Sensitive Detection.- 7.2.3. Direct Methods.- 7.3. Simple Charge Transfer Reactions.- 7.3.1. Reversible Reactions.- 7.3.2. Quasi-Reversible Reactions.- 7.3.3. Irreversible Reactions.- 7.3.4. Second and Higher Harmonics.- 7.3.5. Electrode Growth and Geometry Effects.- 7.4. Coupled Chemical/Electrochemical Processes.- 7.4.1. The CE Mechanism.- 7.4.2. The EC Mechanism.- 7.4.3. The ECE Mechanism.- 7.4.4. The Catalytic Mechanism.- 7.5. Complex Plane Analysis.- 7.6. Faradaic Rectification.- 7.6.1. Alternating Current Control.- 7.6.2. Alternating Potential Control.- 8. Surface Processes.- 8.1. Introduction.- 8.2. Potentiostatic Methods (Chronoamperometry).- 8.2.1. Mechanisms Involving Electrochemically Adsorbed Intermediates.- 8.2.2. Electrocrystallization.- 8.2.3. Film Growth.- 8.3. Galvanostatic Techniques.- 8.3.1. Deposition/Dissolution Processes.- 8.3.2. Passivation and Film Gro