Johannes Fussel – författare
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Häftad, Engelska, 2013
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The present voLume finaLizes the coverage of mononucLear organocopper compounds with Ligands bonded by one carbon atom. As structuraL eLucidation has not yet received much attention in organocopper chemistry and the aggregation of most products is unknown, the term" mononucLear" has been used as expLained in .. Organocopper Compounds" 1, pp. 3/4. Compounds with aLkyL, aLkenyL, and aryL Ligands have aLready been described in VoL- umes 1 (pubLished in 1985) and 2 (pubLished in 1983). The present VoLume 3 contains aLL compounds with aLkynyL, carbonyL, isocyanide, and additionaL Ligands bonded by one carbon atom. The Largest part of this voLume deaLs with copper acetyLides which are wideLy used as reagents in organic syntheses aLthough many of them are onLy poorLy characterized. For abbreviations and dimensions used throughout this voLume, see p. X. Frankfurt, September 1986 Johannes FusseL Remarks on Abbreviations and Dimensions Most compounds and reagents in this volume are presented in tables. Unless otherwise stated, they are arranged in the tables according to the numbers of C atoms in the empirical formula.For the sake of conciseness, some abbreviations are used and some dimensions are omitted in the tables. This necessitates the following clarification. Geometrie isomers are designated according to the IUPAC rules. Structural labels are missing when authors fail to report structural details. Temperatures are given in C, otherwise K stands for Kelvin. Abbreviations used with temperatures are m.p. for melting point, b.p. for boiling point, and dec. for decomposition.
E-bok
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The present volume, "Organoiron Compounds" B 17, systematically covers the literature through the end of 1987 for Sections 1.5.3 to 1.5.3.5, through the end of 1988 for Sections 1.5.4 to 1.5.6.7, and also includes many tater references. This volume continues Se ries B (volumes B 1 to B 15 al ready published) on the mononu clear organoiron compounds; Series A (volumes A 1 to A 9 already published) is devoted to the ferrocenes and Se ries C (volumes C 1 to C 5 and C 7 already published) treats organoiron com pounds with two or more Fe atoms in the molecule. Se ries B thus far includes the following mononuclear organoiron compounds: "Eisen-Organische Verbindungen" B 1 (1976), B 2 (1978, in English), B 3 (1979, partly in English) Sections 1 to 1.1.4.8 on 0 compounds and carbonyl compounds. "Eisen-Organische Verbindungen" B 4 (1978) Sections 1.1.5 to 1.2.3.2.3 on isonitrile and carbene compounds and on compounds with ligands bonded to the Fe atom by two C atoms eL ligands). "Eisen-Organische Verbindungen" B 5 (1978) Sections 1.3 to 1.3.6 on compounds with ligands bonded to the Fe atom by three C atoms (3L ligands).
E-bok
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The present volume finalizes the coverage of organocopper compounds. A complete formula and ligand index for the Gmelin organocopper series will appear shortly as" Organa copper Compounds" 5. The volume describes mononuclear compounds with ligands bonded by two or more carbon atoms as well as all di- to octanuclear and polymeric compounds. Mononuclear compounds with ligands bonded by one carbon atom have already been described in Vol umes 1 (published in 1985), 2 (published in 1983), and 3 (published in 1986). As structural elucidation in organocopper chemistry gained more attention only in the last few years, the terms "mononuclear", "dinuclear" etc. have been used as explained in "Organocopper Compounds" 1, 1985, pp. 3/4: all compounds are treated with their small est formula unit unless a higher nuclearity has been proved. As a consequence, most of the species treated in volumes 1 to 3 are described there because of insufficient structural information although they are alleged not to be monomeric. This way, many of the better characterized compounds appear in the present volume which is reflected by the more than eighty X-ray structure figures. Generally, nuclearity and structure are not only deter mined by the coordination properties of the ligands, but also by steric requirements, and may therefore widely differ for analogous compounds. For abbreviations and dimensions used throughout this volume, see p. X. Frankfurt am Main, July 1987 Johannes Fussel Remarks on Abbreviations and Dimensions Most compounds and reagents in this volume are presented in tables.