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Beskrivning
Reflecting the increased pace of research and the many recent advances in organic chemistry, this series serves as a single-source compendium of the most up-to-date and significant procedures currently in use. Volume 9 consists of checked procedures previously published in annual volumes, revised and updated.
Jeremiah P. Freeman is the editor of Organic Syntheses, Collective Volume 9, published by Wiley.
Innehållsförteckning
Partial table of contents: Synthesis of 2-Substituted Naphthalenediol Derivatives UsingChromium Carbene Complexes:1-Acetoxy-2-Butyl-4-Methoxynaphthalene. Highly Reactive Calcium for the Preparation of OrganocalciumReagents: Preparation of 1-Adamantylcalcium Halides and TheirAddition to Ketones: 1-(1-Adamantyl) Cycohexanol. Bis(Trifluoroethyl)(Carboethoxymethyl)Phosphonate. N-tert--Butoxycarbonyl-2-Bromopyrrole. Allylic Alcohols by Alkene Transfer from Zirconium to Zinc:1-[(tert-Butyldiphenylsilyl)Oxy]-Dec-3-En-5-Ol. 1,3,5-Cyclooctatriene. Diethyl 1-Propyl-2-Oxoethylphosphonate. 3, 4-Diethylpyrrole. Dialkyl Mesoxalates by Ozonolysis of Dialkyl Benzalmalonates:Dimethyl Mesoxalate. Manganese-Copper-Catalyzed Conjugate Addition of OrganomagnesiumReagents to ,beta-Ethylenic Ketones:2-(1,1-Dimethylpentyl)-5-Methyl Cyclohexanone. 4-Dodecylbenzenesulfonyl Azides. Ethyl 2-Methyl-5-Phenyl-3-Furancarboxylate. Preparation and Reactions of Alkenylchromium Reagents:2-Hexyl-5-Phenyl-1-Penten-3-OL. Preparation and Use of (Methoxymethoxy)Methyllithium:1-(Hydroxymethyl) Cycloheptanol. Acetylenic Ethers from Alcohols and Their Reduction to Z- andE-Enol Ethers: 1-Menthoxy-1-Butyne. Methyl 5-Methoxyindole-2-Acetate. A General Method for the Preparation of -Branched Amino Acids:(S)-2-Methyl Proline. Synthesis of Epoxides Using Dimethyldioxirane: trans-StilbeneOxide. Tris(Trimethylsilyl)Silane. Indexes.