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Organic Syntheses, Volume 102
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Beskrivning
The current volume continues the tradition of the Organic Syntheses series, providing carefully checked and edited experimental procedures that describe important synthetic methods, transformations, reagents, and synthetic building blocks or intermediates with demonstrated utility in organic synthesis. These significant and interesting procedures should prove worthwhile to many synthetic chemists working in increasingly diverse areas. A trusted guide for professionals in organic and medicinal chemistry in academia, government, and industries, including pharmaceuticals, fine chemicals, agrochemicals, and biotechnological products.
Produktinformation
- Utgivningsdatum:2026-07-08
- Format:Inbunden
- Språk:Engelska
- Serie:Organic Syntheses
- Antal sidor:736
- Förlag:John Wiley & Sons Inc
- ISBN:9781394452842
Utforska kategorier
Innehållsförteckning
- Sharpless Epoxidation of Divinyl Carbinol 1Klaus-Peter Ruhmann, Paula Mora, and Dirk Trauner*Synthesis of Borane-Ammonia and its Application in the Titanium Tetrachloride Catalyzed Reduction of Carboxylic Acids, Including N-Protected Amino Acids 19Henry J. Hamann, Abdulkhaliq A. Alawaed, and P. Veeraraghavan Ramachandran*Preparation of 1,3-Dihydroxyphenazine 45Trevor Dzwiniel, Emma Markun, James A. Kaduk, Aaron Hollas, Krzystof Pupek, and Nicholas Boaz*A General Method for C-Alkylation of Nitroalkanes with Alkyl Halides: Nickel Photoredox Dual-Catalyzed C-Alkylation of Nitroalkanes 64Sina Rezazadeh, Allyssa M. Conner, and Donald A. Watson*Copper-Catalyzed Suzuki-Miyaura Coupling of Unactivated Alkyl Halides with Arylborons 86Yonglei Zhou, Jian Li, and Weilong Xie*Large-Scale NaBr/Selectfluor Mediated Alcohol Oxidation: Conversion of (-)-Borneol into (-)-Camphor 100Shyam Sathyamoorthi*Photoexcited Nitroarenes for the Anaerobic Cleavage of Alkenes 114Lifeng Yin, Ben S. Kozloff, Ning Deng, Preya D. Persaud, Ajay H. Bansode, Dan E. Wise, Jenny S. Martinez, and Marvin Parasram*C(sp2)-S Cross-Coupling Reactions with Adaptive Dynamic Homogeneous Catalysis: Synthesis of Ethyl 4-((3-Ethoxy-3-oxopropyl)thio)benzoate 128Florence Babawale, Indrajit Ghosh*, and Burkhard König*Preparation of (Z)-N-Phenoxybenzimidoyl Chloride 143Joseph P. Lokant, Ross M. Dare, and David A. Nagib*Synthesis of Serine Derived Oxazolines Using a Molybdenum Dioxide Catalyst 156Wyatt C. Powell, Garrett E. Evenson, and Maciej A. Walczak*Synthesis of 1-(phenylsulfonyl)bicyclo[1.1.0]butane from Methyl Phenyl Sulfone and Epichlorohydrin 185Joanna E. Muir, Myunggi Jung, and Vincent N. G. Lindsay*Iodine-Catalyzed Stereospecific anti-Diamination of trans- -Methylstyrene 203Takeshi Sugiyama, Chiyuki Naito, and Satoshi Minakata*Large-Scale Syntheses of Silanoxy-Tetrahydrofurans via Stereospecific [5,5]-Rearrangements of Silanol Epoxides 217Silver Raju and Shyam Sathyamoorthi*βEfficient Preparation of Chiral Hydroxylamines via Nickel-Catalyzed Asymmetric Hydrogenation of Oximes 236Bowen Li, Jianzhong Chen, and Wanbin Zhang*Rapid Access to Enantiopure Protected (R)-Paraconyl Alcohol 251Haylie E. Hennigan, Namuunzul Otgontseren, and Elizabeth I. Parkinson*EditorialAnnouncing "OS Techniques" - A New Category of Articles in Organic Syntheses 273Rick L. DanheiserOS TechniquesPurification of Organic Compounds by Flash Column Chromatography 276Benjamin D. Senzer, Cholapat Varongchayakul, Rick L. Danheiser*, Brian Daniels, and Vy M. Dong*OS TechniquesGlass Cannula for Bulb-to-Bulb Cold Transfer 303Kaylin N. Flesch, Tyler J. Fulton, Nathan Hart, and Brian M. Stoltz*Synthesis of gem-Difluoroalkenes through Ramberg-Bäcklund Reaction of Alkyltriflones 315Motoo Ohtsuka, Yasuyo Tahara-Tezuka, Yuuki Maekawa, Cathleen M. Crudden*, and Masakazu Nambo*Synthesis of 6-Methoxy-2-methyl-2-(4-methylpent-3-en-1-yl) chroman-4-one via Kabbe Condensation 335Stephen A. Chamness, Emily F. Traficante, Trenton R. Vogel, and Corinna S. Schindler*Preparation of Bu-MsFluind-Br 350Lucas Wagner and Josep Cornella*Synthesis of α-Aryl Ketones via the Nickel-Catalyzed Hydroacylation of Aryl Alkenes with Aroyl Fluorides 367Yoonho Lee, Yujin Jung, Seonhwa Choo, and Kwangmin Shin*Synthesis of meta-Substituted Benzenes via Mo-Catalyzed Intermolecular Deoxygenative Coupling of Ynones and Allylic Amines 381Yi-Zhe Yu, Gang Fang, Hong-Yi Su, and Chun-Xiang Zhuo*Large-Scale Alkene Dimesyloxylation 398Shyam Sathyamoorthi*Acid-Mediated Hydroaminomethylation of Unactivated Alkenes 414Uros Vezonik, Paolo Piacentini and Nuno Maulide*Hydrosilylation of Propiolate Esters 428Allison M. Clark, Giulianna Miseo, and Neil K. Garg*Synthesis of Abietatriene via Nitrogen Deletion 442Julia L. Driscoll, Carys E. Obertone, Liao Chen, and Mark D. Levin*Oxidative Nitrogen Atom Insertion into Cyclopentenones 465Bence B. Botlik and Bill Morandi*Preparation of N-tert-Butylbenzenesulfinimidoyl Chloride 477Teruaki Mukaiyama, Yasuo Nakamura, and Jun-ichi Matsuo*Large-Scale Amino-Hydroxylation Using Tethered Nitreniums 494Shyam Sathyamoorthi*Discussion Addendum:Nickel-Catalyzed Synthesis of Ketones from Alkyl Halides and Acid Chlorides: Preparation of Ethyl 4-Oxododecanoate 512Omar M. Beleh and Daniel J. Weix*Synthesis of 4,4-Dimethyl-1,6-Heptadiyne and Derivatives from Dimedone 534Amir Tavakoli, Nathaniel J. Selvaraj, and Gregory B. Dudley*Preparation of S-Trifluoromethyl Trifluoromethanesulfonothioate (TTST), a Highly Versatile and Atom-economical Trifluoromethylthiolating Agent 562Seyedesahar Miraghaee, Teruo Umemoto, and Gerald B. Hammond*Palladium-Catalyzed Carbonylative Spirolactonization of Hydroxycyclopropanols 582Cyrus C. Gudeman, Courtney M. Wiethorn, and Mingji Dai*Umpolung Synthesis of α-Bromo Secondary Amides from Unactivated Hydroxamates 601Rui Wang, Hao Cao, and Wenbo H. Liu*Enzymatic Saponification of Esters Containing β-Leaving Groups 625Benjamin A. Janda, Allison M. Clark, and Neil K. Garg*Preparation of Hexafluoroisopropyl Sulfamate (HFIPS) for the Sulfamoylation of Alcohols and Amines 637Mathew L. Piotrowski, Matthew Sguazzin, Jarrod W. Johnson, and Jakob Magolan*Preparation of (S,S)-B2bg2, a Chiral Diboron Reagent 657Cliff Yang, Brooklyn Maddox, Anshu Yadav, and Robert E. Maleczka Jr.*