Crystal Structure Analysis

Graduate students, lecturers, and professionals in crystallography, solid state chemistry, condensed matter physics, structural biology, and materials science, will find the thrust of this book exciting ... Professionals in the field would be morally and professionally remiss if they failed to read, consult and discuss this volume with students and colleagues. Amongst several features contributing towards making the book an important acquisition are: comprehensive and up-to-date character; emphasis on practical aspects of the topic; inclusion of many worked examples and problems; and an abundance of illustrative material throughout.

• Preface ; Acknowledgements ; 1. A basic introduction to x-ray crystallography ; 2. Crystal growth, evaluation and mounting ; 3. Symmetry and space group determination ; 4. Background theory for data collection ; 5. Data collection using four-circle diffractometers ; 6. Area detectors ; 7. Fourier syntheses ; 8. Structure determination by Patterson methods ; 9. Direct methods of crystal structure determination ; 10. An introduction to maximum entropy ; 11. Least squares fitting of parameters ; 12. Practical aspects of structure refinement ; 13. The derivation of results ; 14. The interpretation of results ; 15. The presentation of results ; 16. The Crystallographic Information File (CIF) ; 17. Crystallographic databases ; 18. Other topics ; A. Useful mathematics and formulae ; B. A short crystallographic dictionary ; C. Answers to the exercises