Christopher J. Moody - Böcker

The definitive guide to the principles and practice of experimental organic chemistry — fully updated and now featuring more than 100 experimentsThe latest edition of this popular guide to experimental organic chemistry takes students from their first day in the laboratory right through to complex research procedures. All sections have been updated to reflect new techniques, equipment and technologies, and the text has been revised with an even sharper focus on practical skills and procedures.The first half of the book is devoted to safe laboratory practice as well as purification and analytical techniques; particularly spectroscopic analysis. The second half contains step-by-step experimental procedures, each one illustrating a basic principle, or important reaction type. Tried and tested over almost three decades, over 100 validated experiments are graded according to their complexity and all are chosen to highlight important chemical transformations and to teach key experimental skills.New sections cover updated health and safety guidelines, additional spectroscopic techniques, electronic notebooks and record keeping, and techniques, such as semi-automated chromatography and enabling technologies such as the use of microwave and flow chemistry. New experiments include transition metal-catalysed cross-coupling, organocatalysis, asymmetric synthesis, flow chemistry, and microwave-assisted synthesis. Key aspects of this third edition include: Detailed descriptions of the correct use of common apparatus used in the organic laboratoryOutlines of practical skills that all chemistry students must learnHighlights of aspects of health and safety in the laboratory, both in the first section and throughout the experimental proceduresFour new sections reflecting advances in techniques and technologies, from electronic databases and information retrieval to semi-automated chromatographyMore than 100 validated experiments of graded complexity from introductory to research levelA user-friendly experiment directoryAn instructor manual and PowerPoint slides of the figures in the book available on a companion websiteA comprehensive guide to contemporary organic chemistry laboratory principles, procedures, protocols, tools and techniques, Experimental Organic Chemistry, Third Edition is both an essential laboratory textbook for students of chemistry at all levels, and a handy bench reference for experienced chemists.

Neutral reactive intermediates - radicals, carbenes, nitrenes, and arynes - have an interesting place within the history of organic chemistry. Once regarded as curiosities, then intensively studied from the mechanistic point of view by physical organic chemists, they now play a key role in synthetic chemistry. This concise text concentrates on the last aspect of reactive intermediate chemistry; the important reactions of these electron-deficient species are laid out clearly and simply, with carefully chosen examples illustrating their use in organic synthesis. Each chapter includes a few problems as well as suggestions for further reading and provides undergraduates with an invaluable summary of this important topic in organic chemistry.

Experimental Organic Chemistry, Fourth Edition – back cover copy The definitive guide to the principles and practice of experimental organic chemistry — fully updated and now featuring 106 experiments. The latest edition of this popular guide to experimental organic chemistry takes students from their first day in the laboratory right through to complex research procedures. All sections have been thoroughly updated to reflect new techniques, equipment and technologies. The first half of the book is devoted to safe laboratory practice as well as purification and analytical techniques; particularly spectroscopic analysis. The second half contains step-by-step experimental procedures, each illustrating a basic principle, or important reaction type. Tried and tested over almost four decades, the 106 validated experiments are graded according to their complexity, and all are chosen to highlight important chemical transformations and to teach key experimental skills. The fourth edition text has been revised with a sharper focus on sustainability, removing halogenated solvents where possible, alongside a brief discussion on the use of artificial intelligence (AI) within research. New experiments cover continuous flow photochemistry and mechanochemistry. Key aspects of the fourth edition include: Detailed descriptions of the correct use of common apparatus used in the organic chemistry laboratoryThorough consideration of health and safety in the laboratory throughout Updated sections on electronic laboratory notebooks (ELN) and record keeping, archival of electronic information, online searching, and the development of modern techniques such as benchtop NMR spectroscopy and 15N, 31P, and 19F NMR spectroscopy.106 validated experiments of graded complexity from introductory to research level.A user-friendly experiment directoryAn Instructor’s Manual and PowerPoint slides of the figures in the book available on a companion websiteAccompanied by a Workbook with a comprehensive set of more than 300 problems and solutions designed to illustrate and develop the themes of each of the 106 experiments A comprehensive guide to contemporary organic chemistry laboratory principles, procedures, protocols, tools and techniques, Experimental Organic Chemistry, Fourth Edition is both an essential laboratory textbook for students of chemistry at all levels, and a handy bench reference for experienced chemists.