NMR of Quadrupolar Nuclei in Solid Materials

AvRoderick E. Wasylishen,Sharon E. Ashbrook

Inbunden, Engelska, 2012

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Beskrivning

NMR OF QUADRUPOLAR NUCLEI IN SOLID MATERIALS Over the past 20 years technical developments in superconducting magnet technology and instrumentation have increased the potential of NMR spectroscopy so that it is now possible to study a wide range of solid materials. In addition, one can probe the nuclear environments of many other additional atoms that possess the property of spin. In particular, it is possible to carry out NMR experiments on isotopes that have nuclear spin greater that ½ (i.e. quadrupolar nuclei). Since more that two-thirds of all NMR active isotopes are quadrupolar nuclei, applications of NMR spectroscopy with quadrupolar nuclei are increasing rapidly. The purpose of this handbook is to provide under a single cover the fundamental principles, techniques and applications of quadrupolar NMR as it pertains to solid materials. Each chapter has been prepared by an expert who has made significant contributions to out understanding and appreciation of the importance of NMR studies of quadrupolar nuclei in solids. The text is divided into three sections: The first provides the reader with the background necessary to appreciate the challenges in acquiring and interpreting NMR spectra of quadrupolar neclei in solids. The second presents cutting-edge techniques and methodology for employing these techniques to investigate quadrupolar nuclei in solids. The final section explores applications of solid-state NMR studies of solids ranging from investigations of dynamics, characterizations of biological samples, organic and inorganic materials, porous materials, glasses, catalysts, semiconductors and high-temperature superconductors. About EMR Handbooks The Encyclopedia of Magnetic Resonance (EMR) publishes a wide range of online articles on all aspects of magnetic resonance in physics, chemistry, biology and medicine. The existence-of this large number of articles, written by experts in various fields, is enabling the publication of a series of EMR Handbooks on specific areas of NMR and MRI. The chapters of each of these handbooks will comprise a carefully chosen selection of Encyclopedia articles. In consultation with the EMR Editorial Board, the EMR Handbooks are coherently planned in advance by specially-selected Editors, and new articles, are written (together with updates of some already existing articles) to give appropriate complete coverage. The handbooks are intended to be of value and interest to research students, postdoctoral fellows and other researchers learning about the scientific area in question and undertaking relevant experiments, whether in academia or industry. Have the content of this handbook and the complete content of the Encyclopedia of Magnetic Resonance at your fingertips! Visit: www.wileyonlinelibrary.com/ref/emr

Produktinformation

Utgivningsdatum:2012-06-15
Mått:196 x 254 x 28 mm
Vikt:1 356 g
Format:Inbunden
Språk:Engelska
Serie:eMagRes Books
Antal sidor:560
Förlag:John Wiley & Sons Inc
ISBN:9780470973981

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Mer om författaren

Roderick E. Wasylishen, Canada Research Chair in Physical Chemistry, Department of Chemistry, Edmonton, Alberta, Canada. Sharon E. Ashbrook, Reader, School of Chemistry, University of St Andrews, UK. Stephen Wimperis, Professor, Department of Chemistry, Faculty of Physical Sciences, University of Glasgow, UK.

Innehållsförteckning

Contributors ixSeries Preface xiiiVolume Preface xvPart A: Basic Principles 11 Quadrupolar InteractionsPascal P. Man 32 Quadrupolar Nuclei in SolidsAlexander J. Vega 173 Quadrupolar Coupling: An Introduction and Crystallographic AspectsSharon E. Ashbrook, Stephen Wimperis 454 Quadrupolar Nuclei in Solids: Influence of Different Interactions on SpectraDavid L. Bryce, Roderick E. Wasylishen 63Part B: Advanced Techniques 755 Acquisition of Wideline Solid-State NMR Spectra of Quadrupolar NucleiRobert W. Schurko 776 Sensitivity and Resolution Enhancement of Half-Integer Quadrupolar Nuclei in Solid-State NMRThomas T. Nakashima, Roderick E. Wasylishen 957 Quadrupolar Nutation SpectroscopyArno P.M. Kentgens 1078 Dynamic Angle SpinningPhilip J. Grandinetti 1219 Double Rotation (DOR) NMRRay Dupree 13310 MQMAS NMR: Experimental StrategiesJean-Paul Amoureux, Marek Pruski 14311 STMAS NMR: Experimental AdvancesSharon E. Ashbrook, Stephen Wimperis 16312 Correlation Experiments Involving Half-Integer Quadrupolar NucleiMichael Deschamps, Dominique Massiot 17913 Computing Electric Field Gradient TensorsJosef W. Zwanziger 199Part C: Applications 21114 Quadrupolar NMR to Investigate Dynamics in Solid MaterialsLuke A. O’Dell, Christopher I. Ratcliffe 21315 Alkali Metal NMR of Biological MoleculesGang Wu 23316 Nitrogen-14 NMR Studies of Biological SystemsLuminita Duma 25517 Oxygen-17 NMR Studies of Organic and Biological MoleculesGang Wu 27318 Oxygen-17 NMR of Inorganic MaterialsSharon E. Ashbrook, Mark E. Smith 29119 Chlorine, Bromine, and Iodine Solid-State NMRDavid L. Bryce, Cory M. Widdifield, Rebecca P. Chapman, Robert J. Attrell 32120 Quadrupolar NMR of Ionic Conductors, Batteries, and other Energy-Related MaterialsFrédéric Blanc, Leigh Spencer, Gillian R. Goward 34921 Quadrupolar NMR of Nanoporous MaterialsMohamed Haouas, Charlotte Martineau, Francis Taulelle 37122 Quadrupolar NMR in the Earth SciencesJonathan F. Stebbins 38723 Quadrupolar NMR of SuperconductorsNicholas J. Curro 40124 Quadrupolar NMR of SemiconductorsJames P. Yesinowski 41725 Quadrupolar NMR of Metal Nuclides in Biological MaterialsTatyana Polenova, Andrew S. Lipton, Paul D. Ellis 43926 Nuclear Waste Glasses: Insights from Solid-State NMRScott Kroeker 45327 Quadrupolar Metal NMR of Oxide Materials Including CatalystsOlga B. Lapina, Victor V. Terskikh 46728 Quadrupolar NMR of Intermetallic CompoundsFrank Haarmann 495Index 511